Instrumentation

Shimadzu GC-2010

  • Injector: Temperature-programmable on-column
  • Detector: Flame Ionization Detector (FID) Capillary Column
  • Restek Rtx®-5, 10m, 0.32mm (id), 0.10µm
  • Guard Column: -5m x 0.53mm (id) Data Handling Software
  • PeakSimple Chromatography® Software

Analytical Conditions

  • Inlet: On-column, 1µL (Note: Immediately after injection, the inlet is programmed to follow the temperature program of the oven.)
  • Detector: FID, 380°C
  • Oven:
  • 50°C (1 min)
    1. @ 15°C/min to 180°C
    2. @ 7°C/min to 230°C
    3. @ 30°C/min to 380°C (10 min)
  • Carrier Gas: Helium, 3 mL/min